Síntese orgânica de 1,4-benzoxazepinas heterocíclicas

Síntese orgânica de 1,4-benzoxazepinas heterocíclicas

Abdellah Echchahad / BRAHIM EL GHMARI / HANANE FARAH

65,43 €
IVA incluido
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Editorial:
KS OmniScriptum Publishing
Año de edición:
2026
ISBN:
9786209573538
65,43 €
IVA incluido
Disponible

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Sobre IBD

Este estudo centra-se na reatividade do 2 -aminobenzilálcool em relação a epóxidos geminados (dicianos e cianoésteres) que se comportam como bi-electrofílicos. O método permite a síntese de 1,4-benzoxazepin-3-onas com um rendimento muito elevado através da abertura simples do epóxido seguida de ciclização. Todos os produtos são caracterizados em pormenor por RMN, espetrometria de massa e espetrometria de infravermelhos com transformada de Fourier (FT-IR). Com os ciano-ésteres (2), o método permite a produção de novas 1,4-benzoxazepinas através de uma reação eficiente num único local, sem a necessidade de um catalisador. Simples de executar, seletivo e realizável em condições suaves, este método abre novas perspectivas na química medicinal, com o objetivo de conceber novos compostos bioactivos.

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