Organische Synthese der heterocyclischen Produkte 1,4-Benzoxazepine

Organische Synthese der heterocyclischen Produkte 1,4-Benzoxazepine

Abdellah Echchahad / BRAHIM EL GHMARI / HANANE FARAH

65,43 €
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Editorial:
KS OmniScriptum Publishing
Año de edición:
2026
ISBN:
9786209560736
65,43 €
IVA incluido
Disponible

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Die Studie konzentriert sich auf die Reaktivität von 2-Aminobenzylalkohol gegenüber bifunktionalisierten gem - Epoxiden (Dicyano und Cyano-Ester), die sich gleichzeitig als bi-elektrophil verhalten. Die Methode ermöglicht eine sehr effiziente Synthese von 1,4-Benzoxazepin-3-onen in sehr hoher Ausbeute durch eine einfache Epoxidöffnung mit anschließender Zyklisierung. Alle Produkte werden durch NMR, Massenspektrometrie und Fourier-Transformierte Infrarot-Spektrometrie (FTIR) bis ins kleinste Detail charakterisiert. Bei den Cyano-Estern (2) ermöglicht die Methode die Herstellung von 1,4-Benzoxazepinen, die durch eine effiziente Ein-Topf-Reaktion ohne Katalysator als neuartig gelten. Die Methode ist einfach durchzuführen, selektiv und unter milden Bedingungen durchführbar und bietet neue Perspektiven für die medizinische Chemie, um neue bioaktive Verbindungen zu entwickeln.

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