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Synteza tytanianu

Synteza tytanianu

Elson Longo / Renata da Silva Magalhães / Silvio r. teixeira

41,51 €
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Editorial:
KS OmniScriptum Publishing
Año de edición:
2025
Materia
Empresa y gestión
ISBN:
9786208633486
41,51 €
IVA incluido
Disponible

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Sobre IBD

Tytaniany baru (BT) i strontu (ST) zostały wytworzone przy użyciu dwóch różnych metod, reakcji w stanie stałym (SSR), w temperaturach 1150/1200°C i hydrotermalnej wspomaganej mikrofalami (MAH), z różnymi stężeniami mineralizatora KOH (1, 3 i 6 mol/L). Chlorek baru i strontu oraz TiO2 w fazie anatazu zostały użyte jako prekursory w procesie przygotowania metodą SSR. W syntezach prowadzonych metodą MAH zastosowano te same chlorki, a jako prekursor tytanu wykorzystano kompleks anatazu z nadtlenkiem wodoru. We wszystkich preparatach otrzymano tytaniany, ale z różnymi wynikami pod względem krystalizacji i morfologii cząstek, co może być związane z różnymi stężeniami mineralizatora, rodzajem użytego prekursora tytanu i zastosowaniem różnych strategii syntezy. Materiały powstałe w wyniku obu procesów zostały scharakteryzowane za pomocą dyfraktometrii rentgenowskiej (XRD), spektroskopii mikro-Ramana (MR), spektroskopii w podczerwieni z transformacją Fouriera (FTIR), UV-Vis, skaningowej mikroskopii elektronowej (SEM), a na koniec zarejestrowano ich emisję fotoluminescencyjną (FL).

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